Abstract: This new type nanocomposite powder was prepared with electroless plating enhanced by ultrasonic wave. High-resolution transmission electron microscopy (HRTEM) showed that As-plated particles have nano meter scale average size. X-ray diffraction (XRD) analysis showed the presence of a noncrystalline structure in the plating layer on the nano-Al₂O₃ matrix. The content of the plating layer was analyzed by energy disper sive X-ray spectroscopy (EDX) technology. The plating layer content was adjustable by changing the solution concentration.

Key words: nanocomposite powder, Al₂0₃ nanoparticles, electroless plating enhanced with ultrasonic wave

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