Full Text:   <2416>

Summary:  <1987>

CLC number: TQ051.13

On-line Access: 2017-04-05

Received: 2017-02-15

Revision Accepted: 2017-02-20

Crosschecked: 2017-03-09

Cited: 0

Clicked: 3831

Citations:  Bibtex RefMan EndNote GB/T7714

 ORCID:

Jing-dai Wang

http://orcid.org/0000-0003-2229-9034

-   Go to

Article info.
Open peer comments

Journal of Zhejiang University SCIENCE A 2017 Vol.18 No.4 P.245-255

http://doi.org/10.1631/jzus.A1700082


From noise to information: a new technology of olefin polymerization fluidized bed reactor based on acoustic emission


Author(s):  Hao-tong Wang, Zheng-liang Huang, Zu-wei Liao, Bin-bo Jiang, Jing-dai Wang, Yong-rong Yang, Guo-dong Han, Bao-zhu Yang

Affiliation(s):  State Key Laboratory of Chemical Engineering & Department of Chemical and Biological Engineering, Zhejiang University, Hangzhou 310027, China; more

Corresponding email(s):   wangjd@zju.edu.cn

Key Words:  Fluidized bed, Acoustic emission, Agglomeration, Meso-scale, Scale-up


Share this article to: More |Next Article >>>

Hao-tong Wang, Zheng-liang Huang, Zu-wei Liao, Bin-bo Jiang, Jing-dai Wang, Yong-rong Yang, Guo-dong Han, Bao-zhu Yang. From noise to information: a new technology of olefin polymerization fluidized bed reactor based on acoustic emission[J]. Journal of Zhejiang University Science A, 2017, 18(4): 245-255.

@article{title="From noise to information: a new technology of olefin polymerization fluidized bed reactor based on acoustic emission",
author="Hao-tong Wang, Zheng-liang Huang, Zu-wei Liao, Bin-bo Jiang, Jing-dai Wang, Yong-rong Yang, Guo-dong Han, Bao-zhu Yang",
journal="Journal of Zhejiang University Science A",
volume="18",
number="4",
pages="245-255",
year="2017",
publisher="Zhejiang University Press & Springer",
doi="10.1631/jzus.A1700082"
}

%0 Journal Article
%T From noise to information: a new technology of olefin polymerization fluidized bed reactor based on acoustic emission
%A Hao-tong Wang
%A Zheng-liang Huang
%A Zu-wei Liao
%A Bin-bo Jiang
%A Jing-dai Wang
%A Yong-rong Yang
%A Guo-dong Han
%A Bao-zhu Yang
%J Journal of Zhejiang University SCIENCE A
%V 18
%N 4
%P 245-255
%@ 1673-565X
%D 2017
%I Zhejiang University Press & Springer
%DOI 10.1631/jzus.A1700082

TY - JOUR
T1 - From noise to information: a new technology of olefin polymerization fluidized bed reactor based on acoustic emission
A1 - Hao-tong Wang
A1 - Zheng-liang Huang
A1 - Zu-wei Liao
A1 - Bin-bo Jiang
A1 - Jing-dai Wang
A1 - Yong-rong Yang
A1 - Guo-dong Han
A1 - Bao-zhu Yang
J0 - Journal of Zhejiang University Science A
VL - 18
IS - 4
SP - 245
EP - 255
%@ 1673-565X
Y1 - 2017
PB - Zhejiang University Press & Springer
ER -
DOI - 10.1631/jzus.A1700082


Abstract: 
The fluidized bed is widely used in many industrial processes because of its vigorous mixing and heat transfer properties. However, when heat transfer is blocked, the particles are easily melted and agglomerated, and even cause the industrial reactor to shut down. From the point of mechanism analysis, the process of explosive agglomeration is a typical meso-scale problem in the fluidized bed, and there is a complex evolution process between particle fluidization and reactor shutdown. Grasping the regulation of meso-scale structure is one of the major challenges faced by chemical engineering. Thus, in this background, the fluidized bed acoustic emission detection technology, agglomeration fault self-repair technology, and a direct scale-up technique of the fluidized bed mathematical model were invented. These technologies have provided strong reliability for stable operation and have been successfully applied in 14 sets of industrial plants.

从噪声到信息:基于声发射监控的聚烯烃流化床反应器新技术

目的:在全球所有的合成树脂中,聚烯烃的产能位居榜首,在国民经济建设和社会发展中发挥着重要作用。但流化床聚合反应器内的高静电会引起颗粒团聚,一旦传热受阻,颗粒极易熔融结块,甚至导致装置爆聚停车。本研究旨在针对流化床聚合反应过程具有强放热、高静电、变粒径的特点,提出基于声发射技术的多种检测手段和信息提取方法。
创新点:针对聚合过程的爆聚结块问题,本研究主要解决了以下难题:(1)流化床内颗粒和结块的原位表征技术缺失,难以检测;(2)颗粒熔融结块过程的在线干预机制不清楚,难以调控;(3)流动传热过程强耦合,反应器放大规律不明,导致反应器难放大等问题。
方法:创立声发射信号的多尺度解析方法,通过小波分解和重标极差分析法分类重构将声发射信号分解为微尺度、介尺度和宏尺度信号;提出基于声发射检测的反应器操作优化技术,并通过建模确立流化床聚合反应器的时空产率数学模型。
成果:新技术成功应用于"十一五"国家重点建设项目--天津百万吨乙烯工程相配套的年产30万吨气相法聚乙烯流化床反应器的设计建设。并且,新技术已成功应用于14套大型聚烯烃装置的设计或改造,所涉及的聚乙烯产能达263万吨。作者所在团队也因该技术发明获得了2016年度国家技术发明奖二等奖。

关键词:流化床;声发射;聚团;介尺度;放大

Darkslateblue:Affiliate; Royal Blue:Author; Turquoise:Article

Reference

[1]Han, G.D., Wang, J.D., Chen, M., et al., 2015. An On-line Cleaning Method for Producing a Low-density Polyethylene Gas-phase Fluidized Bed Reaction System. China Patent 105237665A (in Chinese).

[2]He, L.L., Yang, Y., Huang, Z., et al., 2016. Multi-scale analysis of acoustic emission signals in dense-phase pneumatic conveying of pulverized coal at high pressure. AIChE Journal, 62(8):2635-2648.

[3]He, Y.J., Wang, J.D., Cao, Y.J., et al., 2009. Resolution of structure characteristics of AE signals in multiphase flow system—from data to information. AIChE Journal, 55(10):2563-2577.

[4]Jiang, X.J., Wang, J.D., Jiang, B.B., et al., 2007. Study of the power spectrum of acoustic emission (AE) by accelerometers in fluidized beds. Industrial & Engineering Chemistry Research, 46(21):6904-6909.

[5]Maucci, E., Briens, C., Martinuzzi, R., et al., 1999. Detection and characterization of piston flow regime in three-phase fluidized beds. Powder Technology, 103(3):243-259.

[6]Ren, C.J., Wang, J.D., Yang, Y.R., 2008. Acoustic emission signal analysis of particle motion and the fluidization condition judgement in the gas solid fluidized bed. Science China B: Chemistry, 38(7):645-651.

[7]Ren, C.J., Tang, Y.Q., Wang, J.D., et al., 2011. Online estimation of coke in a circulating fluidized bed based on acoustic emission sensors and multivariate calibration. Industrial & Engineering Chemistry Research, 50(14):8420-8429.

[8]Wang, F., Wang, J.D., Yang, Y.R., 2008. Distribution of electrostatic potential in a gas-solid fluidized bed and measurement of bed level. Industrial & Engineering Chemistry Research, 47(23):9517-9526.

[9]Wang, J.D., Yang, Y.R., Ge, P.F., et al., 2007. Experimental research of multiscale resolution of acoustic emission and fluidization velocity in the gas solid fluidized bed. Science China B: Chemistry, 37(1):94-100.

[10]Wang, J.D., Yang, Y.R., Cao, Y.J., et al., 2008a. Determination of dew point in gas phase fluidized bed of condensed mode. China Patent 101140264A (in Chinese).

[11]Wang, J.D., Yang, Y.R., Ren, C.J., et al., 2008b. A Detection Method for Distribution Plate in a Fluidized Bed Reactor. China Patent 101226169A (in Chinese).

[12]Wang, J.D., Cao, Y.J., Jiang, X.J., et al., 2009a. Agglomeration detection by acoustic emission (AE) sensors in fluidized beds. Industrial & Engineering Chemistry Research, 48(7):3466-3473.

[13]Wang, J.D., Ren, C.J., Yang, Y.R., et al., 2009b. Characterization of particle fluidization pattern in a gas solid fluidized bed based on acoustic emission (AE) measurement. Industrial & Engineering Chemistry Research, 48(18):8508-8514.

[14]Wang, J.D., Ren, C.J., Yang, Y.R., 2010. Characterization of flow regime transition and particle motion using acoustic emission measurement in a gas-solid fluidized bed. AIChE Journal, 56(5):1173-1183.

[15]Wang, J.D., Lou, J.M., Sun, J.Y., et al., 2011. A Detection Method for Liquid Atomization Condition. China Patent 102262040A (in Chinese).

[16]Wang, J.D., Zhu, Z.C., Wu, J.T., et al., 2012. A Pre-distributor for Gas Feed in a Fluidized Bed Reactor. China Patent 102350275A (in Chinese).

[17]Wu, W.Q., Yang, Y.R., Wang, J.D., et al., 2013. Composite Catalyst for Production of Polyethylene. US Patent 8536286.

[18]Yang, Y.R., Hou, L.X., Yang, B.Z., et al., 2003. Device and Methods for Sound Wave Monitoring of Fluidized Bed Reactors. China Patent 1544140A (in Chinese).

[19]Yang, Y.R., Hou, L.X., Hu, X.P., et al., 2004. A Gas Distribution Plate for the Fluidized Bed Reactor. China Patent 1481930A (in Chinese).

[20]Yang, Y.R., Hou, L.X., Wang, J.D., et al., 2005. Multi-scale resolve of acoustic signal and experimental investigation of particle size distribution. Progress in Natural Science, 15(3):380-384.

[21]Yang, Y.R., Wang, J.D., Jiang, B.B., et al., 2006. A Detection Method for Fluidized Bed Reactor. China Patent 1831494 (in Chinese).

[22]Yang, Y.R., Wu, W.Q., Luo, G.H., et al., 2008. Development and Device of Condensate Introduction to the Polymerization Fluidized Bed. China Patent 101284889A (in Chinese).

[23]Yang, Y.R., Wang, J.D., Huang, Z.L., et al., 2009. An Anti-explosion Type Electrostatic Detection Device in the Fluidized Bed. China Patent 100562753C (in Chinese).

[24]Zhao, G.B., Yang, Y.R., 2003. Multiscale resolution of fluidized bed pressure fluctuations. AIChE Journal, 49(4):869-882.

[25]Zhou, Y.F., Dong, K.Z., Huang, Z.L., et al., 2011. Fault detection based on acoustic emission–early agglomeration recognition system in fluidized bed reactor. Industrial & Engineering Chemistry Research, 50(14):8476-8484.

Open peer comments: Debate/Discuss/Question/Opinion

<1>

Please provide your name, email address and a comment





Journal of Zhejiang University-SCIENCE, 38 Zheda Road, Hangzhou 310027, China
Tel: +86-571-87952783; E-mail: cjzhang@zju.edu.cn
Copyright © 2000 - 2024 Journal of Zhejiang University-SCIENCE