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Cleaner and convenient preparation of 3-(4,6-dimethoxy-pyrimidin-2-yloxy)-2-methyl-phenol
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WEN Yue-zhong, FANG Zhao-hua, LIU Wei-ping. Cleaner and convenient preparation of 3-(4,6-dimethoxy-pyrimidin-2-yloxy)-2-methyl-phenol[J]. Journal of Zhejiang University Science A, 2004, 5(8): 956-959.
@article{title="Cleaner and convenient preparation of 3-(4,6-dimethoxy-pyrimidin-2-yloxy)-2-methyl-phenol",
author="WEN Yue-zhong, FANG Zhao-hua, LIU Wei-ping",
journal="Journal of Zhejiang University Science A",
volume="5",
number="8",
pages="956-959",
year="2004",
publisher="Zhejiang University Press & Springer",
doi="10.1631/jzus.2004.0956"
}
%0 Journal Article
%T Cleaner and convenient preparation of 3-(4,6-dimethoxy-pyrimidin-2-yloxy)-2-methyl-phenol
%A WEN Yue-zhong
%A FANG Zhao-hua
%A LIU Wei-ping
%J Journal of Zhejiang University SCIENCE A
%V 5
%N 8
%P 956-959
%@ 1869-1951
%D 2004
%I Zhejiang University Press & Springer
%DOI 10.1631/jzus.2004.0956
TY - JOUR
T1 - Cleaner and convenient preparation of 3-(4,6-dimethoxy-pyrimidin-2-yloxy)-2-methyl-phenol
A1 - WEN Yue-zhong
A1 - FANG Zhao-hua
A1 - LIU Wei-ping
J0 - Journal of Zhejiang University Science A
VL - 5
IS - 8
SP - 956
EP - 959
%@ 1869-1951
Y1 - 2004
PB - Zhejiang University Press & Springer
ER -
DOI - 10.1631/jzus.2004.0956
Abstract: Environmental concerns have highlighted the need of cleaner technologies. A cleaner, convenient and selective technology has been developed for the preparation of 3-(4,6-dimethoxy-pyrimidin-2-yloxy)-2-methyl-phenol (DPMP) from 2-methyl-benzene-1,3-diol in water as solvent. The isolated yield of DPMP is up to 86% in good selectivity. The product structure was characterized by conventional methods, 1H-NMR and MS. This technology belongs to the modern concept of environmentally friendly low wastes or non-wastes technology (LWNWT).
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