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Journal of Zhejiang University SCIENCE A 2004 Vol.5 No.4 P.428-431

http://doi.org/10.1631/jzus.2004.0428


Solid-phase microextraction for flavor analysis in Harari Khat (Catha edulis) stimulant


Author(s):  AL-FLAHI Abdulsalam, ZOU Jian-kai, YIN Xue-feng

Affiliation(s):  Department of Chemistry, Zhejiang University, Hangzhou 310027, China

Corresponding email(s):   Flahi2@yahoo.com, jklj@mail.hz.zj.cn, cheyinxf@mail.hz.zj.cn

Key Words:  Solid-phase microextraction, Gas chromatography-mass spectrometry, Catha, Khat leaves, Khat in Yemen, Chat (Khat) in Ethiopia


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AL-FLAHI Abdulsalam, ZOU Jian-kai, YIN Xue-feng. Solid-phase microextraction for flavor analysis in Harari Khat (Catha edulis) stimulant[J]. Journal of Zhejiang University Science A, 2004, 5(4): 428-431.

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author="AL-FLAHI Abdulsalam, ZOU Jian-kai, YIN Xue-feng",
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doi="10.1631/jzus.2004.0428"
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A1 - AL-FLAHI Abdulsalam
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Abstract: 
This research examined the typical flavor compounds in the commonest type of Khat called Harari Khat grown in the region of Ethiopia. Twenty-eight compounds, which includes 1,2-Propanedione, 1-Phenyl, Hexanol, Hexanal compounds, Limonene, Benzaldehyde with other flavors, were extracted by polydimethylsiloxane at room temperature for 30 min from Khat samples, and identified by solid-phase microextraction-gas chromatography-mass spectrometry (SPME-GC-MS). This method needs no organic solvents and required minimal sample.

Darkslateblue:Affiliate; Royal Blue:Author; Turquoise:Article

Reference

[1] Ameen, J.R.M., Naji, J.A., 2001.Causal models for road accident fatalities in Yemen.Accident Analysis Prevention,33:547-561.

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[3] Hattab, F.N.,Birgit, A.M., 2000. Fluoride content in Khat (Catha edulis) chewing leaves. Archives of Oral biology,45:253-255.

[4] Jiu, A., 1997. Headspace solid-phase microextraction dynamics and quantitative analysis before reaching a partition equilibrium.Anal. Chem,69:3260-3266

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[6] Jon, G.W., Eric. D.C., Yongkyoung, K., Manuel, H., John, B.S., Dwight, W.M., 2000. Sample preparation for the analysis of flavors and off-flavor in foods.Journal of Chromatography:A,880:3-33.articls

[7] Lewis, L., 1931. Phantastica, Narcotic and Stimulating Drugs (Translation of 1924, German edition). Routle and Kegan Paul, London.

[8] Pawliszyn, J., 1999. Application of Solid Phase Microextraction (Book), Chapters 1 & 2 on Quantitation.Royal Society of Chemistry,85:404-525.

[9] Ripani, L., Schiavone, S., Garofano, L., 1996. GC/MS identification ofcatha edutisstimulant-active.Forensic Science International,78:39-46.

[10] Yang, X., Peppard, T., 1994. Solid-phase microextraction for flavor analysis.J. Agric. Food Chem.,42:1925-1930.

[11] Yang, S.S., Huang, C.B., Smetena, I., 2002. Microextraction for volatile compounds in Tobacco.Journal of Chromatography:A,942:33-39.

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ZIKI@Colas<cziki2002@yahoo.co.uk>

2010-11-19 00:55:21

good article

C Ziki<cziki2002@yahoo.co.uk>

2010-11-19 00:54:10

good article - i need first to read the full text

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