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Received: 2003-07-07

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Journal of Zhejiang University SCIENCE A 2004 Vol.5 No.6 P.705-708

http://doi.org/10.1631/jzus.2004.0705


Rapid synthesis of ZSM-5 zeolite catalyst for amination of ethanolamine


Author(s):  HUA Yue-ming, HU Wang-ming

Affiliation(s):  Department of Chemical Engineering, Zhejiang University, Hangzhou 310027, China

Corresponding email(s):   huwm@zju.edu.cn

Key Words:  ZSM-5 zeolite, Synthesis, Pretreatment, Alkalinity


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HUA Yue-ming, HU Wang-ming. Rapid synthesis of ZSM-5 zeolite catalyst for amination of ethanolamine[J]. Journal of Zhejiang University Science A, 2004, 5(6): 705-708.

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author="HUA Yue-ming, HU Wang-ming",
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pages="705-708",
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publisher="Zhejiang University Press & Springer",
doi="10.1631/jzus.2004.0705"
}

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%A HU Wang-ming
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%I Zhejiang University Press & Springer
%DOI 10.1631/jzus.2004.0705

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T1 - Rapid synthesis of ZSM-5 zeolite catalyst for amination of ethanolamine
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Abstract: 
ZSM-5 zeolite was rapidly synthesized in system containing ethylenediamine from the initial gel: (5-8) Na2O: 44 EDA:Al2O3:100 SiO2:4000 H2O. The crystals were lath-shaped. The effect of pretreatment and alkalinity on crystallinity was investigated. The pretreatment of silicate source can cut down the crystallization time. Tuning the system alkalinity and controlling crystallization time can ensure forming of pure crystal.

Darkslateblue:Affiliate; Royal Blue:Author; Turquoise:Article

Reference

[1] Davis, M.E., 1998. Zeolite-based catalysts for chemical synthesis.Microporous and Mesoporous Materials,21(4-6):173-182.

[2] Hu, J.X., Li, Y.W., Xiang, H.W., Xu, Y.Y, He, L.M, Gao, M.X., 2001.The Method of Rapidly Synthesizing Small Crystalline ZSM-5 Zeolite with Template Agent. CN00109593.5 (in Chinese).

[3] Hua, Y.M., Hu, W.M., 2001. Synthesis of ethylenediamines over ZSM-5 zeolite.Hua Xue Shi Jie,42(9):480 (in Chinese).

[4] Li, H.Y., Liang, J., Ying, M.L., 1983. Synthesis of ZSM-5 zeolite of high silica/alumina ratio.Cui Hua Xue Bao,4(3):244-247 (in Chinese).

[5] Liu, M., Xiang, S.H., 2001. Studies on the synthesis of zeolite ZSM-5 with different morphology and crystal size.Shi You Xue Bao(Shi You Jia Gong),17(2):24-29 (in Chinese).

[6] Zhang, C.L., Kan, Q.B., Wu, Z.Y., 1995. Rapid synthesis and characterization of Fe-ZSM-5 zeolite.Shi You Xue Bao(Shi You Jia Gong),11(4):20-26 (in Chinese).

Open peer comments: Debate/Discuss/Question/Opinion

<1>

bintang@UI<bintangmahaputra@live.com>

2012-03-18 18:55:02

i am very gratfeul if you could send me this paper to my email. thanks a lot

bintang@No address<bintangmahaputra@live.com>

2012-03-18 18:53:51

i am very grateful if you could send me this paper to my email. thanks a lot

faisal@No address<FAISAL.JUHANI.1@ARAMCO.COM>

2012-01-17 18:19:23

could you please send me this paper for refrence

H. Mahmoudi@PhD Sutdent<hmahmoudi@gmail.com>

2012-01-15 05:05:52

I will be grateful if you kindly send me the paper for referencing.

Bridget Egbi Nwobi@Ahmadu Bello University Zaria Nigeria<bnwobi2002@yahoo.com>

2011-03-16 05:33:22

i am a PhD student of the above institute and am working on the synthesis of zsm5. i will be very grateful if you can send me this paper for referencing

Abebe@KTH<endalew@gmial.com>

2010-12-24 18:51:38

thanks

indah@undip<lover.comp@gmail.com>

2010-11-20 15:22:34

i want download this paper for my reference.... thanks...

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